| Anmol Chemicals is the pioneer manufacturers of Saccharin Sodium Saccharin Calcium n Saccharin Insoulble, Pharmaceutical Excipients Food & Flavor chemicals in India. We supply Halal and Kosher Saccharin Sodium Saccharin made in an ISO9001, ISO22000 (FSSC22000) cGMP and GLP certified facility. Our group has several manufacturing facilities spread across the world, supported by toll manufacturers and representatives in UAE, Europe, USA, China and has several associated manufacturing facilities spread across India. All the Information on Physics, Chemistry, Applications, Uses and Technology on Manufacture of Saccharin Sodium is in these pages. |
| The units have one or more of the certifications like FDA GMP, ISO 9001, ISO 22000, HACCP, REACH, Kosher & Halal |
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Saccharin Sodium BP EP Ph Eur USP NF FCC Food Grade Manufacturers
Saccharin Sodium CAS Number 82385-42-0 & 128-44-9, EINECS EC Number 204-886-1, HS Code ---**; Molecular Weight 205.17 anhydrous, Molecular Formula: C7H4NNaO3S-xH2O
Specifications of Saccharin Sodium BP EP Ph EUR USP NF FCC Food Grade Manufacturers; YOU ARE HERE
Specifications of Saccharin Calcium USP NF FCC Food Grade Manufacturers
Specifications of Saccharin Insoluble BP EP Ph Eur USP NF FCC Food Grade Manufacturers
Saccharin Sodium SDS MSDS Sheet of Manufacturers
Saccharin is primarily produced in two types i.e. soluble and insoluble saccharin. The soluble saccharin (in water) is called Sodium Saccharin whereas insoluble saccharin is called Insoluble Saccharin.
Saccharin is produced in two physical forms, viz granular and powder
Saccharin is used in a variety of industry such as food and beverage, personal care products, table top sweetener, electroplating brighteners, pharmaceuticals etc.
Calcium Saccharin, is also sometimes used, especially by people restricting their dietary sodium intake. Calcium Saccharin is a sweeteners that has been used in food for many years. In cosmetics and personal care products, Calcium Saccharin is used as flavoring agents in the formulation of dental products, mouthwashes and lipstick.
General Specifications of Sodium Saccharin or Soluble Saccharin:
Description: White crystalline powder or colorless crystals; efflorescent in dry air.
CAS Number 82385-42-0]
Chemical Name: Sodium salt of1,2-benzisothiazolin-3-one 1,1-dioxide.
Molecular Formula: C7H4NNaO3S
Molecular Weight: 205.19
Solubility: Freely soluble in water; sparingly soluble in ethanol(95%); practically insoluble in ether.
Identification: The infra red spectrum of the substance being examined should be concordant with the reference spectrum.
Melting range: 226 -230C
Heavy metals: Not more than 20 ppm.
OTS Amide content: Not more than 25 ppm
Water content by KF: 12.0 – 16.0%w/w.
Assay: Not less than 98.0% and not more than 101.0%on Anhydrous basis.
Saccharin Sodium BP EP Ph Eur USP NF is also offered. As per the monograph of Saccharin Sodium BP EP Ph Eur its content analyses between 99 to 101% assay and meets the requirement of trace impurities specified in the monograph.
Saccharin Sodium BP Grade
Soluble Saccharin
Ph Eur
C7H4NNaO3S - 205.2 - CAS Number 128-44-9
Action and use: Sweetening agent.
DEFINITION
2-Sodio-1,2-benzisothiazol-3(2H)-one 1,1-dioxide.
Content: 99.0 per cent to 101.0 per cent (anhydrous substance). It may contain a variable quantity of water.
CHARACTERS
Appearance: White or almost white, crystalline powder or colourless crystals, efflorescent in dry air.
Solubility: Freely soluble in water, sparingly soluble in ethanol (96 per cent).
IDENTIFICATION
First identificationiB, E.
Second identificationiA, C, D, E.
A. Melting point: 226C to 230C.
To 5 ml of solution S (see Tests) add 3 ml of dilute hydrochloric acid. A white precipitate is formed. Filter and wash with water. Dry the precipitate at 100-105 °C.
B. Infrared absorption spectrophotometry.
C. Mix about 10 mg with about 10 mg of resorcinol, add 0.25 ml of sulphuric acid and carefully heat the mixture over a naked flame until a dark green colour is produced. Allow to cool, add 10 ml of water and dilute sodium hydroxide solution until an alkaline reaction is produced. An intense green fluorescence develops.
D. To 0.2 g add 1.5 ml of dilute sodium hydroxide solution, evaporate to dryness and heat the residue carefully until it melts, avoiding carbonisation. Allow to cool, dissolve the mass in about 5 ml of water, add dilute hydrochloric acid until a weak acid reaction is produced and filter, if necessary. To the filtrate add 0.2 ml of ferric chloride solution. A violet colour develops.
E. Solution S gives reaction (a) of sodium.
TESTS
Solution S: Dissolve 5.0 g in carbon dioxide-free water and dilute to 50.0 ml with the same solvent.
Appearance of solution: The solution is clear and colourless.
Dissolve 5.0 g in 25 ml of carbon dioxide-free water.
Acidity or alkalinity: To 10 ml of solution S add about 0.05 ml of a 10 g/l solution of phenolphthalein in ethanol (96 per cent). The solution is not pink. Add 0.1 ml of sodium hydroxide 0.1 M. The solution becomes pink.
o- and p-Toluenesulphonamide: Gas chromatography to pass the test.
Readily carbonisable substances: Dissolve 0.20 g in 5 ml of sulphuric acid and keep at 48-50C for 10 min. When viewed against a white background, the solution is not more intensely coloured than a solution prepared by mixing 0.1 ml of red primary solution, 0.1 ml of blue primary solution and 0.4 ml of yellow primary solution with 4.4 ml of water.
Heavy metals: Maximum 20 ppm.
Water: Maximum 15.0 per cent, determined on 0.200 g.
ASSAY
Dissolve 0.150 g in 50 ml of anhydrous acetic acid, with slight heating if necessary. Titrate with 0.1 M perchloric acid, determining the end-point potentiometrically. Carry out a blank titration. 1 ml of 0.1 M perchloric acid is equivalent to 20.52 mg of C7H4NNaO3S.
STORAGE
In an airtight container.
Sodium Saccharin FCC Food Grade
1,2-Benzisothiazole-3(2H)-one 1,1-Dioxide Sodium Salt;
Sodium o-Benzosulfimide; Soluble Saccharin
C7H4NNaO3S·2H2O --- Formula wt 241.19
INS: 954 CAS Number CAS Number 128-44-9
DESCRIPTION
Sodium Saccharin occurs as white crystals or as a white, crystalline powder. In powdered form, it effloresces to the extent that it usually contains only about one-third the amount of water indicated in its molecular formula. One gram is soluble in 1.5 mL of water and in about 50 mL of alcohol.
Function: Nonnutritive sweetener.
REQUIREMENTS
Identification:
A. Dissolve about 100 mg of sample in 5 mL of a 1:20 solution of sodium hydroxide, evaporate to dryness, and gently fuse the residue over a small flame until ammonia no longer evolves. After the residue has cooled, dissolve it in 20 mL of water, neutralize the solution with 2.7 N hydrochloric acid, and filter. Add 1 drop of ferric chloride to the filtrate. A violet color appears.
B. Mix 20 mg of sample with 40 mg of resorcinol, cautiously add 10 drops of sulfuric acid, and heat the mixture in a liquid bath at 200C for 3 min. After cooling, add 10 mL of water and an excess of 1 N sodium hydroxide. A fluorescent green liquid results.
C. The residue obtained by igniting a 2-g sample gives positive tests for Sodium.
D. Add 1 mL of hydrochloric acid to 10 mL of a 1:10 aqueous solution. A crystalline precipitate of saccharin forms. Wash the precipitate well with cold water, and dry at 105C for 2 h. The saccharin thus obtained melts between 226C and 230C.
Assay: Not less than 98.0% and not more than 101.0% of C7H4NNaO3S, calculated on the anhydrous basis.
Alkalinity: Passes test.
Benzoate and Salicylate: Passes test.
Lead: Not more than 2 mg/kg.
Readily Carbonizable: Substances Passes test.
Selenium: Not more than 0.003%.
Toluenesulfonamides: Not more than 0.0025%.
Water: Not more than 15.0%.
Manufacturers
Anmol Chemicals
S-8, SARIFA MANSION, 2ND FLANK ROAD, CHINCHBUNDER, MUMBAI 400009, INDIA
TEL: (OFFICE) 91-22-23770100, 23726950, 23774610, 23723564. FAX: 91-22-23728264
e-mail: anmolc@mtnl.net.in
Exports to USA, Canada, UAE, Dubai, South Africa, Tanzania, Kenya, Nigeria, Egypt, Uganda, Turkey, Mexico, Brazil, Chile, Argentina, Europe Netherlands, Italy, Spain, Germany, Portugal, France, Malaysia, Indonesia, Thailand, Vietnam, Korea, Japan, etc.
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